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| EAK6012 | Derivatization Methods for HPLC and GCMS | 3+0+0 | ECTS:7.5 | | Year / Semester | Fall Semester | | Level of Course | Third Cycle | | Status | Elective | | Department | ANALYTICAL CHEMISTRY IN PHARMACY | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | This course is to teach the derivatization method for HPLC and GCMS. |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Contribution to knowledge of chemistry. | 2,4,10,11 | 1,3,5, | | PO - 2 : | Together with the ability to use knowledge learned in the course. | 2,4,10,11 | 1,3,5, | | PO - 3 : | To analyze the data, the ability to evaluate in relation to the subject Learning and understanding of one another the ability to distinguish what is known varieties of information. | 2,4,10,11 | 1,3,5, | | PO - 4 : | Improving the scientific method and research skills | 2,4,10,11 | 1,3,5, | | PO - 5 : | Oral, written and practical ability to establish a balance between the scientific activities of the course to have a professional qualification and monitoring and interpreting contemporary issues. | 2,4,10,11 | 1,3,5, | | PO - 6 : | Evaluation of the course content, the ability to use current issues. | 2,4,10,11 | 1,3,5, | | PO - 7 : | Contemporary methods, techniques, tools, and analysis of the ability to use the application. | 2,4,10,11 | 1,3,5, | | PO - 8 : | Field related problems to identify, formulate, and solve engineering problems. | 2,4,10,11 | 1,3,5, | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| Derivatization methods and practices for HPLC and GCMS |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | İntroduction | | | Week 2 | HPLC | | | Week 3 | HPLC | | | Week 4 | GCMS | | | Week 5 | GCMS | | | Week 6 | Derivatization | | | Week 7 | Derivatization | | | Week 8 | General and specific derivatization methods for GC-MS analyses | | | Week 9 | Mid-term exam | | | Week 10 | General and specific derivatization methods for GC-MS analyses | | | Week 11 | General and specific derivatization methods for GC-MS analyses | | | Week 12 | General and specific derivatization methods for HPLC analyses | | | Week 13 | General and specific derivatization methods for HPLC analyses | | | Week 14 | General and specific derivatization methods for HPLC analyses | | | Week 15 | General and specific derivatization methods for HPLC analyses | | | Week 16 | End-of-term exam | | | |
| 1 | Toshimasa Toyo'oka, Modern Derivatization Methods for Separation Sciences, Wiley, 1999. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 25/11/2023 | 1 | 30 | | In-term studies (second mid-term exam) | 15 | 10/01/2024 | 1 | 20 | | End-of-term exam | 16 | 15/01/2024 | 1 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 14 | 42 | | Arasınav için hazırlık | 6 | 8 | 48 | | Arasınav | 2 | 1 | 2 | | Dönem sonu sınavı için hazırlık | 7 | 14 | 98 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 192 |
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