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| KIM 374 | Organic Chemistry Lab. - II | 0+0+4 | ECTS:5 | | Year / Semester | Fall Semester | | Level of Course | First Cycle | | Status | Compulsory | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | Face to face, Lab work | | Contact Hours | 14 weeks - 4 hours of laboratory per week | | Lecturer | Prof. Dr. Nuran KAHRİMAN | | Co-Lecturer | PROF. DR. Ahmet DEMİRBAŞ,LECTURER DR. Nuri YILDIRIM,ASSOC. PROF. DR. Yasemin ÜNVER,ASSIST. PROF. DR. Neşe DOĞAN, | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | Application of various techniques, and synthesis |
| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | do neccessary methods in the analysis of organic compounds | 1,2,3,5,6,7 | 1,4 | | LO - 2 : | synthesize a given organic compounds. | 1,2,3,5,6,7 | 1,4 | | LO - 3 : | interprete synthesis and analysis results | 1,2,3,5,6,7 | 1,4 | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| Preparation for laboratory practice, Oxidation reaction: synthesis of benzoic acide , Reduction reaction: synthesis of azoxibenzene, Nucleophylic aliphatic substitution: synthesis of ethyl bromide, Addition to carbon-heteroatom multiple bond: synrthesis urotropin, Molecular rearrangement: synthesis of alpha-methyl indole, Nucleophylic aromatic substitution: synrhesis of iodobenzene, Addition to carbon-carbon multiple bond: synthesis of cyclohexanole, Elimination reaction: cyclohexen, Electrophylic aromatic substitution: synhtesis of o-, p-nitrophenol, Nucleophylic acyl substitution: synthesis of acetoacetic ester. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Arragenment for laboratory, formation of groups anf giving information on experiments | | | Week 2 | Oxidation reaction, synthesis of benzoic acid | | | Week 3 | Reduction Reactions: Synthesis of azoxibenzene | | | Week 4 | Nucleophilic aliphatic substitution: synthesis of ethyl bomide | | | Week 5 | Addition to carbon-heteroatom multiple bonds: synthesis of urotropin | | | Week 6 | Molecular rearragements: synthesis of alfa methyl indole | | | Week 7 | Nucleophilic aromatic substitution: synthesis of iodobenzene | | | Week 8 | Mid-term exam | | | Week 9 | Addition to carbon-carbon multiple bonds: synthesis of cyclohexanol | | | Week 10 | Elimination reactions: synthesis of cyclohexene | | | Week 11 | Electrophilic aromatic substitution: synthesis of o-,p-nitrophenol | | | Week 12 | Nucleophilic acyl substitution: synthesis of acetoacetic acid | | | Week 13 | compensation | | | Week 14 | compensation | | | Week 15 | compensation | | | Week 16 | End-of-term exam | | | |
| 1 | Pavia,D. L., Lampman, G. M. Kriz, G. S. 1976; Introduction to Organic Laboratory Techniques, second edition, New York | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 02.04.2016 | 2 | 50 | | End-of-term exam | 17 | 03.06.2016 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | .5 | 14 | 7 | | Sınıf dışı çalışma | 2 | 14 | 28 | | Laboratuar çalışması | 5 | 14 | 70 | | Arasınav için hazırlık | 5 | 1 | 5 | | Arasınav | 2 | 1 | 2 | | Kısa sınav | .3 | 10 | 3 | | Dönem sonu sınavı için hazırlık | 8 | 1 | 8 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 125 |
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