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GRADUATE INSTITUTE of NATURAL and APPLIED SCIENCES / DEPARTMENT of CHEMISTRY
Doctorate
Course Catalog
www.ktu.edu.tr/chemistry or http://www.ktu.edu.tr/fakulte/fenedb/index
Phone: +90 0462 3772525
FBE
GRADUATE INSTITUTE of NATURAL and APPLIED SCIENCES / DEPARTMENT of CHEMISTRY / Doctorate
Katalog Ana Sayfa
  Katalog Ana Sayfa  KTÜ Ana Sayfa   Katalog Ana Sayfa
 
 
KIM7640METAL DETERMINATION TECH. AND APPLICATION3+0+0ECTS:7.5
Year / SemesterSpring Semester
Level of CourseThird Cycle
Status Elective
DepartmentDEPARTMENT of CHEMISTRY
Prerequisites and co-requisitesNone
Mode of DeliveryFace to face
Contact Hours14 weeks - 3 hours of lectures per week
Lecturer--
Co-LecturerAssoc. Prof. Dr. Celal DURAN
Language of instructionTurkish
Professional practise ( internship ) None
 
The aim of the course:
To learn metal determination methods in samples including various matrix and applicate these methods in Atomic Spectrometry
 
Programme OutcomesCTPOTOA
Upon successful completion of the course, the students will be able to :
PO - 1 : learn the several metal determination techniques 1,21,5
PO - 2 : get extensive information about Atomic Spectrometry11,5
PO - 3 : describe the determination of metals and their applications with Atomic Spectrometric techniques1,21,5
PO - 4 : get information about Absorption and Emission Spectroscopy21,5
PO - 5 : learn calibration graphics, standard addition, working range, limit of detection, limit of quantification, etc. 1,21,5
CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome

 
Contents of the Course
Lambert-Beer Law, Determination Techniques Based Atomic Energy Absorption, Techniques with Flame, Flameless Techniques; Cold Vapour Technique (CV-AAS), Hydride Generation Technique (HG-AAS), Graphite Furnace Technique (GF-AAS), Determination Techniques Based Atomic Energy Emission, Flame Photometry (FF), Flame Atomic Emission Spectrometry (F-AES), Inductively Coupled Plasma - Atomic Emission Spectroscopy (ICP-AES), Sampling and Dissolution/Digestion in Atomic Spectrometric Techniques, Application of Atomic Spectrometric Techniques for Biological, Environment, Solid, and Liquid Samples.
 
Course Syllabus
 WeekSubjectRelated Notes / Files
 Week 1Lambert-Beer Law
 Week 2Determination Techniques Based Atomic Energy Absorption, Techniques with Flame
 Week 3Determination Techniques Based Atomic Energy Absorption, Techniques with Flame
 Week 4Flameless Techniques; Cold Vapour Technique (CV-AAS), Hydride Generation Technique (HG-AAS)
 Week 5Flameless Techniques; Cold Vapour Technique (CV-AAS), Hydride Generation Technique (HG-AAS)
 Week 6Graphite Furnace Technique (GF-AAS)
 Week 7Determination Techniques Based Atomic Energy Emission, Flame Photometry (FF), Flame Atomic Emission Spectrometry (F-AES)
 Week 8Inductively Coupled Plasma - Atomic Emission Spectroscopy (ICP-AES)
 Week 9 Exam
 Week 10Inductively Coupled Plasma - Atomic Emission Spectroscopy (ICP-AES)
 Week 11Sampling and Dissolution/Digestion in Atomic Spectrometric Techniques
 Week 12Sampling and Dissolution/Digestion in Atomic Spectrometric Techniques
 Week 13Application of Atomic Spectrometric Techniques for Biological, Environment, Solid, and Liquid Samples
 Week 14Application of Atomic Spectrometric Techniques for Biological, Environment, Solid, and Liquid Samples
 Week 15Application of Atomic Spectrometric Techniques for Biological, Environment, Solid, and Liquid Samples
 Week 16End-of-term exam
 
Textbook / Material
1Dulski, T.R. 1999; Trace Elemental Analysis of Metals: Methods and Techniques, New York
 
Recommended Reading
1Dean, J.R. 2003, Methods for Environmental Trace Analysis, John Wiley & Sons, England
2Stoeppler, M. 1992; Hazardous Metals in the Environment, New York
3Cantle, J.E. 1982; Atomic Absorption Spectrophotometry, Techniques and Instrumentation in Analytical Chemistry, New York
 
Method of Assessment
Type of assessmentWeek NoDate

Duration (hours)Weight (%)
Mid-term exam 9 19/11/2012 2 50
End-of-term exam 17 14/01/2013 2 50
 
Student Work Load and its Distribution
Type of workDuration (hours pw)

No of weeks / Number of activity

Hours in total per term
Yüz yüze eğitim 3 14 42
Sınıf dışı çalışma 5 13 65
Ödev 4 12 48
Dönem sonu sınavı için hazırlık 15 2 30
Dönem sonu sınavı 2 1 2
Diğer 1 5 2 10
Diğer 2 2 1 2
Total work load199