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| KIM7762 | Nmr Spectroscopy | 3+0+0 | ECTS:7.5 | | Year / Semester | Spring Semester | | Level of Course | Third Cycle | | Status | Elective | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | Prof. Neslihan DEMIRBAŞ, Prof. Ahmet DEMIRBAŞ, Assoc. Prof. Kemal SANCAK, Assist. Prof. Neşe DOĞAN | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | The use of NMR for structure elucidation. |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Learn magnetic properties of nucleus. | 1,2,3 | 1,3 | | PO - 2 : | Learn NMR instrumentation and technique. | 1,2,3 | 1,3 | | PO - 3 : | Identify the organic structure by NMR | 1,2,3 | 1,3 | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| Introduction, Basic principles, magnetic properties of nucleus, nuclear resonance, nuclear relaxation, NMR instrumentation and technique, chemical shift, spin-spin splitting, interpretation of NMR spectra, applications of NMR to quantitative analysis, NMR spectroscopy of the nuclei other than proton, special topics. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Introduction | | | Week 2 | Basic principles | | | Week 3 | magnetic properties of nucleus | | | Week 4 | nuclear resonance | | | Week 5 | nuclear relaxation | | | Week 6 | NMR instrumentation and technique | | | Week 7 | chemical shift | | | Week 8 | spin-spin splitting | | | Week 9 | Mid-term exam | | | Week 10 | interpretation of NMR spectra | | | Week 11 | applications of NMR to quantitative analysis | | | Week 12 | NMR spectroscopy of the nuclei other than proton | | | Week 13 | Exam | | | Week 14 | Special topics | | | Week 15 | special topics | | | Week 16 | End-of-term exam | | | |
| 1 | Balcı, M. 2000; Nükleer Manyetik Rezonans Spektroskopisi, METU. | | | |
| 1 | Field, L.D. , Sternhell, S. ,Kalman, J. R. 2002; Organic Structures from Spectra, 3rd Edition. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 12/11/2013 | 2 | 30 | | In-term studies (second mid-term exam) | 12 | 21.11.2013 | 2 | 20 | | End-of-term exam | 16 | 07/01/2014 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 13 | 39 | | Sınıf dışı çalışma | 5 | 13 | 65 | | Arasınav için hazırlık | 5 | 2 | 10 | | Arasınav | 2 | 1 | 2 | | Ödev | 1 | 1 | 1 | | Kısa sınav | 2 | 1 | 2 | | Dönem sonu sınavı için hazırlık | 2 | 2 | 4 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 125 |
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