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| KIML7663 | Spectroscopic Special of Phthalocyanines. | 3+0+0 | ECTS:7.5 | | Year / Semester | Spring Semester | | Level of Course | Third Cycle | | Status | Elective | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | Gaining some basic information about the structural characterization of synthesized phthalocyanines. |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Describe the types of spectroscopy | 1,2,3 | | | PO - 2 : | Explain the structures of phthalocyanine compounds using spectroscopic methods | 1,2,3 | | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| Dfinition of phthalocyanine, definition of spectroscopy, types of spectroscopy, characterization methods, IR spectra of phthalocyanines, 1H-NMR spectra of phthalocyanines, 13C-NMR spectra of phthalocyanines, UV-Vis spectra of phthalocyanines, MS spectrum of phthalocyanines |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Introduction, General aspects | | | Week 2 | Definition of spectroscopy | | | Week 3 | Types of spectroscopy | | | Week 4 | Infrared spectroscopy | | | Week 5 | Nuclear magnetic resonance spectroscopy | | | Week 6 | Proton NMR spectroscopy | | | Week 7 | Carbon NMR spectroscopy | | | Week 8 | UV-Vis spectroscopy | | | Week 9 | Midterm Exam | | | Week 10 | IR spectra of phthalocyanines | | | Week 11 | 1H-NMR spectra of phthalocyanines | | | Week 12 | 1H-NMR spectra of phthalocyanines | | | Week 13 | 13C-NMR spectra of phthalocyanines | | | Week 14 | UV-Vis spectra of phthalocyanines | | | Week 15 | Mass spectra of phthalocyanines | | | Week 16 | Final exam | | | |
| 1 | D. Parker, Macrocycle Synthesis, A Practical Approach, Oxford Univarsity Press, 1996. | | | |
| 1 | C.C. Leznoff, Phthalocyanines, Properties and Applications, York University Press, 1993. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 25.11.2021 | 1 | 30 | | In-term studies (second mid-term exam) | 13 | 20.12.2021 | 1 | 20 | | End-of-term exam | 16 | 18.01.2022 | 1 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 13 | 39 | | Sınıf dışı çalışma | 5 | 75 | 375 | | Arasınav için hazırlık | 2 | 8 | 16 | | Arasınav | 1 | 1 | 1 | | Ödev | 2 | 10 | 20 | | Kısa sınav | 1 | 1 | 1 | | Dönem sonu sınavı için hazırlık | 2 | 10 | 20 | | Dönem sonu sınavı | 1 | 1 | 1 | | Total work load | | | 473 |
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