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GRADUATE INSTITUTE of NATURAL and APPLIED SCIENCES / DEPARTMENT of CHEMISTRY
Doctorate
Course Catalog
www.ktu.edu.tr/chemistry or http://www.ktu.edu.tr/fakulte/fenedb/index
Phone: +90 0462 3772525
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GRADUATE INSTITUTE of NATURAL and APPLIED SCIENCES / DEPARTMENT of CHEMISTRY / Doctorate
Katalog Ana Sayfa
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KIM7183The Characterization of Phthalocyanine Struct3+0+0ECTS:7.5
Year / SemesterSpring Semester
Level of CourseThird Cycle
Status Elective
DepartmentDEPARTMENT of CHEMISTRY
Prerequisites and co-requisitesNone
Mode of Delivery
Contact Hours14 weeks - 3 hours of lectures per week
LecturerProf. Dr. Halit KANTEKİN
Co-LecturerNone
Language of instructionTurkish
Professional practise ( internship ) None
 
The aim of the course:
Establishing the correlation between the molecular structure of stable macrocyclic phthalocyanine compounds with technological application and their application areas.
 
Programme OutcomesCTPOTOA
Upon successful completion of the course, the students will be able to :
PO - 1 : Learn effect over colorfulness of pi electron delocalization.1,2,31
PO - 2 : Learn effect on phthalocyanine solubility of substitue groups.1,2,31
PO - 3 : Laern exhibit changing electronik effect on molecule symmetry of phthalocyanine.1,2,31
CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome

 
Contents of the Course
Phatlonitriles, which are used as precursors in the synthesis of metal-free and metallated phthalocyanines, recognition of the chemical structures of metal-free and metalic phthalocyanines, examination of some definitions and concepts in the field of phthalocyanine chemistry.
 
Course Syllabus
 WeekSubjectRelated Notes / Files
 Week 1The purification of phthalocyanine and metallo phthalocyanines with different izolation methods
 Week 2The purification of phthalocyanine and metallo phthalocyanines with different izolation methods
 Week 3The purification of phthalocyanine and metallo phthalocyanines with different izolation methods
 Week 4Characterization with electronic, spectroscopy technique of the structures that containing symetric and asymetric substitue groups bearing to central phthalocyanine ring.
 Week 5Characterization with electronic, spectroscopy technique of the structures that containing symetric and asymetric substitue groups bearing to central phthalocyanine ring.
 Week 6Characterization with 1H-NMR, spectroscopy technique of the structures that containing symetric and asymetric substitue groups bearing to central phthalocyanine ring.
 Week 7Characterization with 1H-NMR, spectroscopy technique of the structures that containing symetric and asymetric substitue groups bearing to central phthalocyanine ring.
 Week 8Mid-term exam
 Week 9Characterization with 13C-NMR, spectroscopy technique of the structures that containing symetric and asymetric substitue groups bearing to central phthalocyanine ring.
 Week 10Characterization with 13C-NMR, spectroscopy technique of the structures that containing symetric and asymetric substitue groups bearing to central phthalocyanine ring.
 Week 11Characterization with IR, spectroscopy technique of the structures that containing symetric and asymetric substitue groups bearing to central phthalocyanine ring.
 Week 12Characterization with IR, spectroscopy technique of the structures that containing symetric and asymetric substitue groups bearing to central phthalocyanine ring.
 Week 13Exam 2
 Week 14Characterization with mass, spectroscopy technique of the structures that containing symetric and asymetric substitue groups bearing to central phthalocyanine ring.
 Week 15Characterization with mass, spectroscopy technique of the structures that containing symetric and asymetric substitue groups bearing to central phthalocyanine ring.
 Week 16End-of-term exam
 
Textbook / Material
1Leznoff, C.C., Lever, A.B.P., (1993), Phthalocyanine Properties and Applications, VCH Publishers, USA.
 
Recommended Reading
1Parker, D., (1996), Macrocycle Synthesis. Oxford University Press, UK, 250 s.
 
Method of Assessment
Type of assessmentWeek NoDate

Duration (hours)Weight (%)
Mid-term exam 9 05/04/2016 1.50 30
In-term studies (second mid-term exam) 12 28/04/2016 1,50 20
End-of-term exam 16 24/05/2016 1.50 50
 
Student Work Load and its Distribution
Type of workDuration (hours pw)

No of weeks / Number of activity

Hours in total per term
Yüz yüze eğitim 3 14 42
Arasınav için hazırlık 10 6 60
Arasınav 2 1 2
Ödev 3 1 3
Dönem sonu sınavı için hazırlık 15 6 90
Dönem sonu sınavı 2 1 2
Total work load199