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| KIM7641 | Dissolving and Solubilization | 3+0+0 | ECTS:7.5 | | Year / Semester | Spring Semester | | Level of Course | Third Cycle | | Status | Elective | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | Face to face | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | Doç. Dr. Celal DURAN | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | Review and discussion of general dissolving techniques, improving new approaches for solubilization systems, investigation of new sample dissolving methods. |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | learn the compiled general dissolving techniques. | 1,2 | 1,5 | | PO - 2 : | make a desicion how to dissolve a sample. | 1 | 1,5 | | PO - 3 : | learn and applicate the solubilization methods. | 1,2,3 | 1,5 | | PO - 4 : | think the sample dissolving other than standard dissolving methods. | 1 | 1,5 | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| General dissolving methods, dissolving under atmospheric conditions, wet digestion method, dry ashing method, dissolving at high pressure, dissolving with microwave, dissolving with ultrasonic wave, dissolving with fusion, dissolving with organic solvents, dissolving under supercritical conditions, selection of dissolving method for the purpose, selection of dissolving method for the sample type, sample dissolving other than standard dissolving methods. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | General dissolving methods | | | Week 2 | Dissolving under atmospheric conditions | | | Week 3 | Dissolving under atmospheric conditions | | | Week 4 | Wet digestion method | | | Week 5 | Dry ashing method | | | Week 6 | Dissolving at high pressure | | | Week 7 | Dissolving with microwave | | | Week 8 | Dissolving with ultrasonic wave | | | Week 9 | Mid-term exam | | | Week 10 | Dissolving with fusion | | | Week 11 | Dissolving with organic solvents | | | Week 12 | Dissolving under supercritical conditions | | | Week 13 | Exam | | | Week 14 | Selection of dissolving method for the purpose, selection of dissolving method for the sample type | | | Week 15 | Sample dissolving other than standard dissolving methods | | | Week 16 | End-of-term exam | | | |
| 1 | Mester, Z., Sturgeon, R. E. 2003; Sample Preparation for Trace Element Analysis, Volume 41 (Comprehensive Analytical Chemistry), Amsterdam, Netherlands | | | 2 | Skoog, D. A., West D.M., Holler, F.J., Crouch, S.R. 2004; Analitik Kimya Temel İlkeler, Türkçe Çeviri Ed.; Kılıç E., Yılmaz, H., 8. Baskı, Bilim Yayıncılık, Ankara | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 10/11/2013 | 2 | 30 | | In-term studies (second mid-term exam) | 13 | 15/12/2013 | 2 | 20 | | End-of-term exam | 16 | 05/01/2014 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 14 | 42 | | Sınıf dışı çalışma | 5 | 13 | 65 | | Arasınav için hazırlık | 10 | 2 | 20 | | Arasınav | 2 | 1 | 2 | | Ödev | 4 | 12 | 48 | | Dönem sonu sınavı için hazırlık | 5 | 2 | 10 | | Dönem sonu sınavı | 2 | 1 | 2 | | Diğer 1 | 4 | 2 | 8 | | Diğer 2 | 2 | 1 | 2 | | Total work load | | | 199 |
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