|
|
| KIM7394 | Method Validations in Analytical Chemistry | 3+0+0 | ECTS:7.5 | | Year / Semester | Fall Semester | | Level of Course | Third Cycle | | Status | Elective | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | Face to face | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | Prof.Dr. Münevver Sökmen, Prof.Dr. Mehmet Tüfekçi | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | Learn the statistic parametters |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Learn the importance of validation at analytical chemistry. | 1,2,3 | 1 | | PO - 2 : | explain the statistic parametters. | 1,2,3 | 1 | | PO - 3 : | Apply the statistic parameters. | 1,2,3 | 1 | | PO - 4 : | Utilise the statistic data and discuss the results
| 1,2,3 | 1 | | PO - 5 : | Discuss the validation methods of using method
| 1,2,3 | 1 | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| Types of Errors in Experimental Data, Statistical Tests, Accuracy, Precision, Limit of Detection, Limit of Quantitation, Selectivity, Linearity, Range, Robustness, Ruggedness, Stability. |
| |
| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Types of Errors in Experimental Data, | | | Week 2 | Types of Errors in Experimental Data, | | | Week 3 | Statistical Tests, | | | Week 4 | Accuracy, | | | Week 5 | Precision, | | | Week 6 | Limit of Detection, | | | Week 7 | Limit of Quantitation, | | | Week 8 | Selectivity, | | | Week 9 | Mid-term exam | | | Week 10 | Linearity, | | | Week 11 | Range, | | | Week 12 | Robustness, | | | Week 13 | 2nd exam | | | Week 14 | Ruggedness, | | | Week 15 | Stability. | | | Week 16 | End-of-term exam | | | |
| 1 | Kılıç, E., Yılmaz, H. 2006; Analitik Kimya Temel İlkeler, Bilim Yayınları, Sekizinci Baskı, Ankara | | | |
| 1 | Gündüz, T., 2002; İnstrümental Analiz, Gazi Kitabevi, 6.Baskı, Ankara | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 11/11/2020 | 1 | 50 | | End-of-term exam | 16 | 04/01/2020 | 1 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Ödev | 10 | 5 | 50 | | Diğer 1 | 4 | 2 | 8 | | Total work load | | | 58 |
|