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| KIML5717 | Separation and Enrichment Techniques | 3+0+0 | ECTS:7.5 | | Year / Semester | Fall Semester | | Level of Course | Second Cycle | | Status | Elective | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | Face to face | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | Prof. Dr. Mehmet Tüfekçi, Prof. Dr. Münevver Sökmen,Prof. Dr. Ömer Dalman, Prof. Dr. Ümmühan Ocak, Prof. Dr. Miraç Ocak, Doç. Dr. Celal Duran, Doç. Dr. Hakan Alp, Öğr. Gör. Dr . Sinan Nohut | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | Learning the separation and enrichment processes required prior to analysis |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Learning generel enrinchement methods | | | | PO - 2 : | Learning evaporation and liquid- liquid extraction | | | | PO - 3 : | Learning precipitation, selective solving | | | | PO - 4 : | Understanding electrochemical precipitation | | | | PO - 5 : | Learning sorption, ion exchange and flotation | | | | PO - 6 : | Learning enrichment methods before analysis | | | | PO - 7 : | Learning separation and purification methods | | | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| General methods of enrichment techniques. Evaporation. Liquid-liquid extraction . Precipitation. Selective dissolution . Electrochemical deposition. Sorption and ion-exchange. Flotation. Freezing and zone melting. Enrichment techniques in gas and water analysis . Separation and purification, fractional precipitation , decomposing and dissolving , separation with hydroxide and sulfide , fluxes , extraction methods, ion exchange , supercritical extraction , chromotography. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | general methods of enrichment techniques. | | | Week 2 | Evaporation, Liguid-liquid extraction | | | Week 3 | Precipitation, Selective solving | | | Week 4 | Electrochemical precipitation, Sorption and ion exchange | | | Week 5 | Flotation. Freezing and melting | | | Week 6 | Enrichment techiques in gas and water analysis | | | Week 7 | Separation and purification, Fractional precipitation | | | Week 8 | Digestion before separation | | | Week 9 | Mid-term exam | | | Week 10 | separation with hydroxide and sulfide | | | Week 11 | Melting, extraction methods | | | Week 12 | Ion exchange | | | Week 13 | Electrophorese | | | Week 14 | Supercritical extraction | | | Week 15 | Chromatograpyh | | | Week 16 | Final exam | | | |
| 1 | Kılıç, Esma, Köseoğlu Fitnat, Analitik Kimya 2, Bilim Yayıncılık | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 06/04/2020 | 1 | 50 | | End-of-term exam | 16 | 01/06/2020 | 1 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 14 | 42 | | Sınıf dışı çalışma | 4 | 14 | 56 | | Laboratuar çalışması | 0 | 0 | 0 | | Arasınav için hazırlık | 5 | 8 | 40 | | Arasınav | 1 | 1 | 1 | | Uygulama | 0 | 0 | 0 | | Klinik Uygulama | 0 | 0 | 0 | | Ödev | 1 | 1 | 1 | | Proje | 0 | 0 | 0 | | Kısa sınav | 0 | 0 | 0 | | Dönem sonu sınavı için hazırlık | 6 | 4 | 24 | | Dönem sonu sınavı | 1 | 1 | 1 | | Diğer 1 | 3 | 8 | 24 | | Diğer 2 | 0 | 0 | 0 | | Total work load | | | 189 |
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