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| BTBL7250 | Concentration on Trace Element Analysis | 3+0+0 | ECTS:7.5 | | Year / Semester | Spring Semester | | Level of Course | Third Cycle | | Status | Elective | | Department | DEPARTMENT of FISHERIES TECHNOLOGY ENGINEERING | | Prerequisites and co-requisites | None | | Mode of Delivery | Face to face | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | None | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | Learn to analysis methods of trace metals which shows toxic property at the low concentrations and determination practice field. |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Learn to the concept of trace elements and toxic effects | 1,2,4 | 1 | | PO - 2 : | Method selection for analysis of trace elements and learn of method sensitivity | 3,4 | 1 | | PO - 3 : | Learn to precision work | 3,4,6 | 1 | | PO - 4 : | Learn to basis of spectroscopic methods and the importanence | 1,2,3,4,6 | 1 | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| Importance of trace analysis and method selection, sample collection in trace analysis, sample preparation, data evaluation and calibration, pre-separation and pre-concentration, principal descriptions in separation techniques, high performance liquid chromatography (HPLC), new developments in heavy metal analysis, determination of heavy metals using voltametric technique in sea water latest developments in spectroscopy about rapid analysis, analyses using atomic spectroscopic techniques, overview to preconcentration techniques, working techniques, precipitation and co-precipitation method, electrochemical methods, preconcentration techniques based on sorption, sorbents, properties and preparation, preconcentration based on the extraction methods, flotation methods, ion exchange methods, organic and inorganic ion exchangers, volatization techniques. Trace metal analysis in fisheries. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Sample preparation techniques and seperation in trace metal analysis | | | Week 2 | Sampling, preparation, data interpretation, calibration. | | | Week 3 | Basic concepts of separation techniques. | | | Week 4 | Solid-phase Extraction, Principles of solid-phase extraction. | | | Week 5 | Holding solid-phase extraction mechanisms, Adsorption, Chelating creation (hard cations, cations of medium hardness, soft cations, ion pair, ion exchange), to be used for the selection of Solid Phase. | | | Week 6 | Şelatlaştırıcı as Ditiyokarbomatlar, Solid-phase extraction application types (micro-columns, cartridges and disposable syringes, loaded resin membrane discs). | | | Week 7 | Implementation Steps (conditioning, adsorption, washing, elusyon), Solid-Phase Extraction Advantages Applications, Liquid-Liquid Extraction, Ion Exchange, crash / crash together. | | | Week 8 | Mid-term exam | | | Week 9 | Electrochemical separation, flotation, Evaporation | | | Week 10 | Atomik Spektroskopi( Absorpsiyon kanunları ve atomik absorpsiyon spektroskopisi) | | | Week 11 | High-performance liquid chromatography | | | Week 12 | Homework, Sample solution | | | Week 13 | New developments in the analysis of heavy metal species
| | | Week 14 | Fishing in the trace element analysis | | | Week 15 | Excuse and Conpensation week | | | Week 16 | End-of-term exam | | | |
| 1 | Gündüz,T. 1997; İnstrümental Analiz. Bilge Yayıncılık, 607s, Ankara. | | | 2 | Pereira, M. G., Arruda, M. A. Z., 2003, Trends in Preconcentration Procedures for Metal Determination Using Atomic Spectrometry Techniques: Fundamental Review. Microchim. Acta, 141, 115- 131. | | | 3 | Alkan,A. 2009; Polistiren- Divinilbenzen Kopolimeri Reçinelerin Modifikasyonu ve Eser Elementlerin Önderiştirilmesinde Kullanılabilirliği. Doktora tezi, Samsun. | | | |
| 1 | Atomik Absorpsiyon Spektrometresinde Uygulamalar.1998; Spektroskopi 88 Yaz Okulu, Trabzon | | | 2 | Atomik Absorpsiyon Spektroskopisinin Temelleri. 1998;Spektroskopi 88 Yaz Okulu, Tabzon | | | 3 | Meloan, C.E., 1999. Chemical Separations Principles, Techniques, and Experiments. John Wiley and Sons Ltd. Newyork, 752. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 8 | 03/04/2012 | 21 | 50 | | End-of-term exam | 16 | 01/06/2012 | 0,6 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 14 | 42 | | Sınıf dışı çalışma | 3 | 14 | 42 | | Arasınav için hazırlık | 2 | 10 | 20 | | Arasınav | 2 | 1 | 2 | | Ödev | 6 | 10 | 60 | | Dönem sonu sınavı için hazırlık | 3 | 11 | 33 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 201 |
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