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| EFG5109 | NMR Spectroscopy of Natural Compunds | 3+0+3 | ECTS:7.5 | | Year / Semester | Fall Semester | | Level of Course | Second Cycle | | Status | Elective | | Department | DEPARTMENT of PHARMACOGNOSY | | Prerequisites and co-requisites | None | | Mode of Delivery | Face to face | | Contact Hours | 14 weeks - 3 hours of lectures and 3 hours of laboratory per week | | Lecturer | -- | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | To teach NMR spectroscopy of Natural Compunds. |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | interpret 1H-NMR spectra. | | | | PO - 2 : | interpret 13C-NMR spectra. | | | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| Introduction to the NMR technique which is used to lighten the structure of the natural compounds, magnetic properties of the nucleus, nuclear resonance, nuclear relaxation, NMR apparatus and appliances, chemical shift, spin-spin splitting, NMR spectra interpretation and application of NMR to quantitative analysis, proton NMR spectra, special topics. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Introduction | | | Week 2 | Basic Principles | | | Week 3 | Magnetic properties of nucleus | | | Week 4 | Nuclear resonance | | | Week 5 | Nuclear relaxation. | | | Week 6 | NMR apparatus and appliances. | | | Week 7 | Chemical shifts. | | | Week 8 | Mid-term exam. | | | Week 9 | Spin-spin splitting. | | | Week 10 | NMR spectra interpretation. | | | Week 11 | NMR spectra interpretation. | | | Week 12 | Proton NMR spectra. | | | Week 13 | 13C-NMR spectra. | | | Week 14 | Application of NMR to quantitative analysis. | | | Week 15 | Special topics. | | | Week 16 | Final exam. | | | |
| 1 | Balcı, M. 2000; Nükleer Manyetik Rezonans Spektroskopisi, METU. | | | |
| 1 | Field, L.D. , Sternhell, S. ,Kalman, J. R. 2002; Organic Structures from Spectra, 3rd Edition. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 8 | 18/11/2013 | 2 | 50 | | End-of-term exam | 16 | 06/01/2014 | 3 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 14 | 42 | | Sınıf dışı çalışma | 3 | 15 | 45 | | Arasınav için hazırlık | 3 | 2 | 6 | | Arasınav | 3 | 1 | 3 | | Ödev | 2 | 10 | 20 | | Dönem sonu sınavı için hazırlık | 3 | 3 | 9 | | Dönem sonu sınavı | 3 | 1 | 3 | | Total work load | | | 128 |
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