|
|
| EAK5009 | Analysis Methods in Pharmacy | 3+0+0 | ECTS:7.5 | | Year / Semester | Fall Semester | | Level of Course | Second Cycle | | Status | Elective | | Department | ANALYTICAL CHEMISTRY IN PHARMACY | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | The aim of this course is to teach recent methods for analysis of pharmaceutical active ingredients in pharmaceuticals and biological samples (blood and urine exc.). Thus, students will effectively use these methods used in the industry and scientific laboratories. |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Have information on the analysis methods used for pharmaceutical active substances. | 1,3,9 | 1, | | PO - 2 : | Learn which analysis methods can be effectively used for what kind of drug active substances. | 1,3,9 | 1, | | PO - 3 : | Learn how to make analysis of drug active substances from commercial formulations and biological samples. | 1,3,9 | 1, | | PO - 4 : | Have information on how to interpret of analysis results obtained experimentally. | 1,3,9 | 1, | | PO - 5 : | Learn how to compare these methods using the results obtained from different analysis methods | 1,3,9 | 1, | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| It includes theoretical lectures and presentations of various analysis methods used for drugs in laboratories for analysis (anhydrous titration, water determination methods, polarimetry, refractometry, resolution, determination methods, pKa determination methods). |
| |
| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | General identification of analysis methods used in pharmaceuticals | | | Week 2 | Titration in anhydrous media | | | Week 3 | Theory of water determination methods | | | Week 4 | Application of water determination methods to pharmaceutics and implementation of experimental results | | | Week 5 | Theory of polarimetry | | | Week 6 | Theory of polarimetry | | | Week 7 | Application of polarimetry method to pharmaceutics and implementation of experimental results | | | Week 8 | Theory of refractometry method | | | Week 9 | Mid-term exam | | | Week 10 | Application of refractometry method to pharmaceutics and implementation of experimental results | | | Week 11 | Theory of solubility determination methods
| | | Week 12 | Application of solubility determination methods to pharmaceutics and implementation of experimental results | | | Week 13 | Theory of pKa determination methods | | | Week 14 | Application of pKa determination methods to pharmaceutics and implementation of experimental | | | Week 15 | Summarize of the analysis methods | | | Week 16 | End-of-term exam | | | |
| 1 | Skoog, D.A., Holler, F.J. and Crouch, S.R. (2017) Principal of Instrumental Analysis. 7th Edition, Sunder College Publisher, New York. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 25/11/2023 | 2 | 30 | | In-term studies (second mid-term exam) | 15 | 10/01/2024 | 2 | 20 | | End-of-term exam | 16 | 15/01/2024 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 15 | 45 | | Arasınav için hazırlık | 5 | 8 | 40 | | Arasınav | 2 | 1 | 2 | | Dönem sonu sınavı için hazırlık | 6 | 15 | 90 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 179 |
|