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| EAK5018 | Chromatographic Methods in Drug Analysis | 3+0+0 | ECTS:7.5 | | Year / Semester | Fall Semester | | Level of Course | Second Cycle | | Status | Compulsory | | Department | ANALYTICAL CHEMISTRY IN PHARMACY | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | It aims to teach students chromatographic methods and their use in drug analysis. |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Learns the theory of chromatographic methods. | 1,6,11 | 1,3, | | PO - 2 : | Learns how to analyze drugs using chromatographic methods. | 1,6,11 | 1,3, | | PO - 3 : | Learns how chromatographic methods are used in the field of pharmacy. | 1,6,11 | 1,3, | | PO - 4 : | Follows current studies on this subject by scanning the studies in the literature. | 1,6,11 | 1,3, | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| Description of chromatography, adsorption chromatography, partition chromatography, ion exchange chromatography, gel permeation chromatography, thin layer chromatography, paper chromatography, column chromatography, paper, colon, thin layer chromatography, gas chromatography, high performance liquid chromatography. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Introduction to Chromatography, Chromatography basic concepts | | | Week 2 | Adsorption Chromatography | | | Week 3 | Partition chromatography
| | | Week 4 | Thin layer chromatography
| | | Week 5 | Paper chromatography | | | Week 6 | Column chromatography | | | Week 7 | Ion exchange chromatography | | | Week 8 | Gel permeation chromatography | | | Week 9 | Mid-term exam | | | Week 10 | Gas chromatography | | | Week 11 | Gas chromatography
| | | Week 12 | High performance liquid chromatography (HPLC) | | | Week 13 | High performance liquid chromatography (HPLC)
| | | Week 14 | High performance liquid chromatography (HPLC) | | | Week 15 | Applications of chromatography in drug analysis | | | Week 16 | End-of-term exam | | | |
| 1 | Prof. Dr. Hasan Aydın, Ayırma Metotları, Bizim Büro Yayınevi, Ankara, 2000. | | | 2 | Gündüz, T., İnstrümental Analiz, Gazi Kitabevi, 11. Baskı, Ankara, 2012. | | | |
| 1 | Skoog, D.A., Holler, F.J. and Crouch, S.R. (2017) Principal of Instrumental Analysis. 7th Edition, Sunder College Publisher, New York. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 25/11/2023 | 2 | 30 | | In-term studies (second mid-term exam) | 15 | 10/01/2024 | 2 | 20 | | End-of-term exam | 16 | 15/01/2024 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 15 | 45 | | Arasınav için hazırlık | 3 | 2 | 6 | | Arasınav | 2 | 1 | 2 | | Dönem sonu sınavı için hazırlık | 9 | 15 | 135 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 190 |
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