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| EAK5004 | Electroanalytical Methods in Drug Analysis | 3+0+0 | ECTS:7.5 | | Year / Semester | Fall Semester | | Level of Course | Second Cycle | | Status | Compulsory | | Department | ANALYTICAL CHEMISTRY IN PHARMACY | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | This course aims to teach the students the theory of electroanalytical methods and how drug active ingredients can be analyzed from pharmaceuticals and biological samples (such as blood and urine) using these methods. |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Have information on the electroanalytical analysis methods. | 1,6,11 | 1,3, | | PO - 2 : | Learn how to use which devices. | 1,6,11 | 1,3, | | PO - 3 : | Have information about potantiometric and voltammetric methods. | 1,6,11 | 1,3, | | PO - 4 : | Learn how to analyse drug active ingredients using electroanalytical methods. | 1,6,11 | 1,3, | | PO - 5 : | Have information on how to interpret of analysis results obtained experimentally. | 1,6,11 | 1,3, | | PO - 6 : | Evaluate the results of the analysis to be obtained. | 1,6,11 | 1,3, | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| Theory of electroanalytical methods, introduction of used devices, potentiometric and voltammetric methods and their applications in drug analysis. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Classifications of electroanalytical methods | | | Week 2 | Electrochemical cells, electrode potentials and cell voltage | | | Week 3 | Potential and current calculations | | | Week 4 | Effect of the solution on the electrochemical measurements | | | Week 5 | Current flows and mass transfer in electrochemical cells | | | Week 6 | Identification of working electrodes, reference and indicator electrodes | | | Week 7 | Identification of working electrodes, reference and indicator electrodes | | | Week 8 | Devices used to measure cell potentials | | | Week 9 | Mid-term exam | | | Week 10 | Potentiometric measurements and potentiometric titrations | | | Week 11 | General theory of voltammetric methods | | | Week 12 | Voltammetric methods (linear sweep and cyclic voltammetry, voltammetric pulse methods) | | | Week 13 | Drug analysis by electroanalytical methods | | | Week 14 | Drug analysis by electroanalytical methods | | | Week 15 | Studies and innovations for drug analysis by electroanalytical methods | | | Week 16 | End-of-term exam | | | |
| 1 | Skoog, D.A., Holler, F.J., Nieman, T.A., Çeviri Editörleri: E. Kılıç, F.Köseoğlu, H.Yılmaz. 1992; Enstrümental Analiz İlkeleri, Bilim Yayıncılık. | | | 2 | V. S. Bagotsky (Ed. Niyazi Alper Tapan, Mehmet Levent Aksu). Elektrokimyanın Temelleri, Nobel Akademik Yayıncılık, 2015. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 25/11/2023 | 2 | 30 | | In-term studies (second mid-term exam) | 15 | 04/01/2024 | 1 | 20 | | End-of-term exam | 16 | 15/01/2024 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 14 | 42 | | Arasınav için hazırlık | 8 | 8 | 64 | | Arasınav | 2 | 1 | 2 | | Ödev | 5 | 1 | 5 | | Dönem sonu sınavı için hazırlık | 5 | 15 | 75 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 190 |
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