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| EAK5005 | Spectroscopic Methods in Pharm. Analysis | 3+0+0 | ECTS:7.5 | | Year / Semester | Fall Semester | | Level of Course | Second Cycle | | Status | Compulsory | | Department | ANALYTICAL CHEMISTRY IN PHARMACY | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | -- | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | To provide some theoretical and practical knowledge necessary for Chemistry students who intend to work in the pharmaceutical industry after graduation. |
| Programme Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | PO - 1 : | Has knowledge about the theory of spectroscopic methods. | 1,6,11 | 1,3, | | PO - 2 : | Learns how to perform drug analysis using spectroscopic methods. | 1,6,11 | 1,3, | | PO - 3 : | Learns which analysis can be done with which spectroscopic method. | 1,6,11 | 1,3, | | PO - 4 : | Can scan the literature and follow current studies. | 1,6,11 | 1,3, | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), PO : Learning Outcome | | |
| Spectrophotometric methods used for qualitative and quantitative analysis of drugs in production stages and existing on the market. Measuring drug levels by applying the analysis methods used to various drug active ingredients and biological materials. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Introduction to drug analysis, qualitative and quantitative determination techniques of drugs | | | Week 2 | Spectroscopic methods general concepts | | | Week 3 | Spectroscopic methods general concepts | | | Week 4 | Spectroscopic methods general concepts | | | Week 5 | Atomic spectroscopy and its use in drug analysis | | | Week 6 | Atomic spectroscopy and its use in drug analysis | | | Week 7 | UV-Vis spectroscopy and its use in drug analysis | | | Week 8 | UV-Vis spectroscopy and its use in drug analysis | | | Week 9 | Mid-term exam | | | Week 10 | Fluorescence spectroscopy and its use in drug analysis | | | Week 11 | Fluorescence spectroscopy and its use in drug analysis | | | Week 12 | Mass spectroscopy and its use in drug analysis | | | Week 13 | Mass spectroscopy and its use in drug analysis | | | Week 14 | Spectroscopic surface analysis and its use in pharmacy | | | Week 15 | Spectroscopic surface analysis and its use in pharmacy | | | Week 16 | Final examination | | | |
| 1 | Gündüz, T., İnstrümental Analiz, Gazi Kitabevi, 11. Baskı, 2012. | | | 2 | Tozkoparan, B., Nicel İlaç Analizleri Ders Notları, Hacettepe Üniv. Eczacılık Fak., 2005. | | | 3 | Görög, S., Drug Dafety, Drug Quality, Drug Analysis, Journal of Pharmaceutical and Biomedical Analysis, 2007. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 25/11/2023 | 2 | 30 | | In-term studies (second mid-term exam) | 15 | 10/01/2024 | 2 | 20 | | End-of-term exam | 16 | 15/01/2024 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 14 | 42 | | Arasınav için hazırlık | 8 | 8 | 64 | | Arasınav | 2 | 1 | 2 | | Ödev | 5 | 1 | 5 | | Dönem sonu sınavı için hazırlık | 5 | 15 | 75 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 190 |
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