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| KIM 206 | Analytical Chemistry - II | 4+2+0 | ECTS:6 | | Year / Semester | Spring Semester | | Level of Course | First Cycle | | Status | Compulsory | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | Face to face | | Contact Hours | 14 weeks - 4 hours of lectures and 2 hours of practicals per week | | Lecturer | Prof. Dr. Celal DURAN | | Co-Lecturer | Prof. Mustafa ÖZDEMİR, Assoc. Prof. Miraç OCAK | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | Chemical principles that are particularly important to analytical chemistry. Fundemantal principles of qualitative and quantitative chemical analysis. Theoretical basis of the gravimetric and volumetric analytical methods and some applications. |
| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | describe solutions and indicators for acid/base titrations, derives titration curves. | 1,2,5,6,7,8 | 1 | | LO - 2 : | analyze titration curves for complex acid / base systems. | 2,3,5,6,7,8 | 1 | | LO - 3 : | define titration curves for precipitation and complex formation titrimetry. | 2,3,5,6,7,8 | 1 | | LO - 4 : | solve the electrochemical analyses problems. interprets oxidation-reduction titrations, defines electrochemical cells, solves the problems involving electrode potentials. | 2,3,5,6,7,8 | 1 | | LO - 5 : | calculate standard electrode potentials,
defines thermodynamic potential of electrochemical cells, derives titration curves for redox titration, describe oxidation/reduction indicators.
| 2,3,5,6,7,8 | 1 | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| Acid-Base titration curves, buffer solutions and hydrolysis, poliprotic acids and bases, amphiprotic salts. Titration curves for complex acid-base systems, polyfunctional acids and polyfunctional bases. Application of the neutralization titrations, Reagents used in the preparations of the standard solutions. Complex formation titrations. Complex formation reactions, titrations with aminocarboxylic acids, titrations with inorganic complexing agents. Introduction to electrochemistry: Oxidation-reduction reactions, electrochemical cells, electrode potentials. Cell potentials, calculation of redoxs equilibrium constants, titration curves for redox titrations and indicators. Applications of the oxidation-reduction titrations, oxidazing agents, reducing agents Applications of the oxidation-reduction titrations, oxidation agents, reducing agents. Chemical kinetics |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Titrimetric Methods | | | Week 2 | Acid-Base titration curves | | | Week 3 | Poliprotic acids and bases, amphiprotic salts | | | Week 4 | Application of the neutralization titrations, Reagents used in neutralization titrations
| | | Week 5 | Complex formation titrations, Complex formation reactions, titrations with aminocarboxylic acids, titrations with inorganic complexing agents | | | Week 6 | Introduction to electrochemistry: Oxidation-reduction reactions, electrochemical cells | | | Week 7 | Electrode potentials, Applications of standard electrod potentials | | | Week 8 | Mid-term exam | | | Week 9 | Cell potentials | | | Week 10 | Calculation of redoxs equilibrium constants | | | Week 11 | Titration curves for redox titrations and indicators | | | Week 12 | Applications of the oxidation-reduction titrations | | | Week 13 | Exam | | | Week 14 | Oxidazing and reducing agents | | | Week 15 | Decomposition and dissolution | | | Week 16 | End-of-term exam | | | |
| 1 | Skoog, West, Holler, Crouch, 2004; Analitik Kimya Temel İlkeler, Türkçe Çeviri, Ed. Esma KILIÇ, H. YILMAZ, 8. Baskı, Bilim Yayıncılık, Ankara | | | |
| 1 | Gündüz, T. 1984; Kantitatif Analiz Ders Kitabı, Gazi Yayınevi, Ankara | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 8 | 30/03/2011 | 2 | 30 | | In-term studies (second mid-term exam) | 13 | 02/05/2011 | 2 | 20 | | End-of-term exam | 17 | 24/06/2011 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 6 | 14 | 84 | | Sınıf dışı çalışma | 2 | 14 | 28 | | Arasınav için hazırlık | 8 | 1 | 8 | | Arasınav | 2 | 1 | 2 | | Dönem sonu sınavı için hazırlık | 9 | 2 | 18 | | Dönem sonu sınavı | 2 | 1 | 2 | | Diğer 1 | 8 | 1 | 8 | | Total work load | | | 150 |
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