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| KIM4010 | Method Validation | 2+0+0 | ECTS:4 | | Year / Semester | Spring Semester | | Level of Course | First Cycle | | Status | Elective | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | Face to face | | Contact Hours | 14 weeks - 2 hours of lectures per week | | Lecturer | Prof. Dr. Miraç OCAK | | Co-Lecturer | Prof. Dr. H. Basri Şentürk, Prof. Dr. Mehmet TÜFEKÇİ, Prof. Dr. Ümmühan OCAK, Prof. Dr. Ömer DALMAN, Doç. Dr. Celal DURAN, Doç. Dr. Miraç Ocak, Doç. Dr. Hakan Alp, Öğr. Gör. Dr. Sinan NOHUT | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | To ensure the validity of test results in analytical studies |
| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | Evaluation of the the accuracy of the method | | | | LO - 2 : | Evaluation of the the precision of the method | | | | LO - 3 : |
Know how to report analysis results | | | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| Determination of meaning and importance of method validation, examination of validation parameters and reporting of test results |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | What is method validation? | | | Week 2 | Validation parameters | | | Week 3 | Selectivity / specificity | | | Week 4 | Precision | | | Week 5 | Accuracy | | | Week 6 | Linearty / Linear range | | | Week 7 | Limit of detection | | | Week 8 | Limit of quantification | | | Week 9 | Midterm | | | Week 10 | Repeatability | | | Week 11 | sensitivity | | | Week 12 | robustness | | | Week 13 | Preparation of the rapor | | | Week 14 | Evaluation of analysis results | | | Week 15 | Analiz raporlarının sunumu | | | Week 16 | Final exam | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 07.04.2020 | 1,5 saat | 50 | | End-of-term exam | 16 | 06.06.2020 | 1,5 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 2 | 14 | 28 | | Arasınav için hazırlık | 3 | 8 | 24 | | Arasınav | 1.5 | 1 | 1.5 | | Dönem sonu sınavı için hazırlık | 3 | 5 | 15 | | Dönem sonu sınavı | 1.5 | 1 | 1.5 | | Total work load | | | 70 |
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