|
KIM3004 | Physical Chemistry Laboratory - II | 0+0+2 | ECTS:3 | Year / Semester | Spring Semester | Level of Course | First Cycle | Status | Compulsory | Department | DEPARTMENT of CHEMISTRY | Prerequisites and co-requisites | None | Mode of Delivery | Lab work | Contact Hours | 14 weeks - 2 hours of laboratory per week | Lecturer | Prof. Dr. Sevil SAVAŞKAN YILMAZ | Co-Lecturer | PROF. DR. Selçuk BİLGEN,ASSOC. PROF. DR. Sedat KELEŞ, | Language of instruction | Turkish | Professional practise ( internship ) | None | | The aim of the course: | The course aims to provide the students with a general knowledge on physical chemistry by using some experimental techniques, to enable them to understand how chemical reactions develop to form new chemicals, to help them use their knowledge to understand the some measuring techniques for determination of the physical properties of the solids, liquids and gases, to teach them how to determine the physical and chemical properties of the chemical materials. |
Learning Outcomes | CTPO | TOA | Upon successful completion of the course, the students will be able to : | | | LO - 1 : | apply various theoretical knowledge to practice. | 1,2,3,4,5,6,7,8 | 1,4 | LO - 2 : | describe the chemical and physical techniques for solids, liquids and gaseous materials | 1,2,3,5 | 1,4 | LO - 3 : | apply various measuring and determination techniques in search of physical properties of the materials | 1,2,3,5,6,7 | 1,4 | LO - 4 : | evaluate the results. | 1,2,3,5,6,7,8 | 1,4 | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | |
Determination of cell constantMolecule size determination with measuring of viscosityPotatiometric acid and base titration and determination of Ka constantDetermination of Activity coefficient with glass electrodMeasurement of breaking indexDetermination of KMnO4 by spectrophotometric methodElectrochemistryEtilasetatın sabunlaşma hız sabiti tayiniEffect of temperature on the rate of reactionDetermination of thetartaric acid amount with polarimetric method |
|
Course Syllabus | Week | Subject | Related Notes / Files | Week 1 | Preparatory experiments | | Week 2 | Preparatory experiments | | Week 3 | Cell constant finding | | Week 4 | Viscosity measurements and determination of molecular size | | Week 5 | Potentiometric determination of acid-base titration and constant Ka | | Week 6 | Determination of activity coefficient with glass electrode | | Week 7 | Measurement of refractive index | | Week 8 | Mid-term exam | | Week 9 | Spectrophotometric determination KMnO4 | | Week 10 | Electrochemistry | | Week 11 | Determination of saponification rate constants Etilasetatın | | Week 12 | Examining the effects of temperature on reaction rate | | Week 13 | Polarimetric method for tartaric acid determination | | Week 14 | Problems and solutions related experiments | | Week 15 | Final | | Week 16 | End-of-term exam | | |
1 | Kaygusuz, K., Savaşkan S., Volga C., 2001;Fizikokimya Laboratuvarı-II Deneyleri, KTÜ, Trabzon. | | |
1 | Kaygusuz, K., Büyükkıdan, N. , Sarı, A,1999; Modern Fizikokimya Deneyleri, GOP Üniv. , Tokat. | | 2 | Gürses, A, Bayrakçeken, S. ,1996; Deneysel Fizikokimya, Erzurum. | | |
Method of Assessment | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | Mid-term exam | 9 | 22.04.2022 | 90 dakika | 50 | End-of-term exam | 16 | 17.06.2022 | 90 dakika | 50 | |
Student Work Load and its Distribution | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | Yüz yüze eğitim | .5 | 14 | 7 | Sınıf dışı çalışma | 1 | 14 | 14 | Laboratuar çalışması | 3 | 14 | 42 | Arasınav için hazırlık | 5 | 10 | 50 | Arasınav | 1 | 1 | 1 | Kısa sınav | .5 | 14 | 7 | Dönem sonu sınavı için hazırlık | 15 | 1 | 15 | Dönem sonu sınavı | 1.5 | 1 | 1.5 | Total work load | | | 137.5 |
|