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| KIM2019 | Analytical Chemistry - I | 4+2+0 | ECTS:5 | | Year / Semester | Fall Semester | | Level of Course | First Cycle | | Status | Compulsory | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | Face to face | | Contact Hours | 14 weeks - 4 hours of lectures and 2 hours of practicals per week | | Lecturer | Prof. Dr. Ömer DALMAN | | Co-Lecturer | Prof. Dr. Miraç Ocak, Prof.Dr. Ömer DALMAN, Prof.Dr. Ümmühan OCAK, Prof.Dr. Celal DURAN and Assoc. Prof. Hakan Alp | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | Chemical principles that are particularly important to analytical chemistry. Fundamental principles of qualitative and quantitative chemical analysis. Theoretical basis of the gravimetric and volumetric analytical methods and some applications. |
| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | explain the fundamentals of analytical chemistry and steps of a characteristic analysis. | 1,2,3,4,5,6,7,8 | 1 | | LO - 2 : | evaluate the analytical data in terms of statistics. | 1,2,3,4,5,6,7,8 | 1 | | LO - 3 : | do basic calculations in analytical methods. | 1,2,3,4,6,7,8 | 1 | | LO - 4 : | identify quality of experimental measurements. | 1,2,3,4,5,6,7,8 | 1 | | LO - 5 : | define the different gravimetric and titrimetric methods. | 1,2,3,4,5,6,7,8 | 1 | | LO - 6 : | interpret the data related to aqueous solution chemistry. | 1,2,3,4,5,6,7,8 | 1 | | LO - 7 : | apply the equilibrium calculations to complex systems. | 1,2,3,4,5,6,7,8 | 1 | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| Introduction to analytical chemistry, Importance and role of analytical chemistry in science, Classifications of analytical methods, Chemistry of aqueous solutions, Chemical equilibrium, Effect of electrolytes on ionic equilibria, Thermodynamic and concentration equilibrium constants, Activitiy and activity coefficients, Complex equilibria systems and calculation of solubility problems in complex systems, Separations of ions by precipitating agent, Gravimetric methods, Calculation of the gravimetric measurements, Properties of precipitates and precipitating agents, Introduction to titrimetric analysis. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Introduction to Analytical Chemistry, Basic Concepts, Analytical Chemistry Tools | | | Week 2 | Calculations in Analytical Chemistry | | | Week 3 | Aqueous Solutions and Chemical Equilibria | | | Week 4 | Aquous Solution Chemistry and Their Constituents | | | Week 5 | Effect of Electrolytes on Chemical Equlibria | | | Week 6 | Effect of Electrolytes on Ionic equilibria | | | Week 7 | Thermodynamic and Concentration Equilibrium Constants | | | Week 8 | Activitiy and Activity Coefficients | | | Week 9 | Mid-term exam | | | Week 10 | Equilibria in Complex Systems | | | Week 11 | Applications of Equilibrium Calculations in Complex Systems, Solution Methods of Mutli-equilibrium Problems | | | Week 12 | Calculation of Solubility Equilibrium | | | Week 13 | Gravimetric methods: Calculation of the Gravimetric Measurements, Properties of Precipitates and Precipitating Agents | | | Week 14 | Introduction to Titrimetric Analysis | | | Week 15 | Volumetric calculations, Precipitation titrations | | | Week 16 | End-of-term exam | | | |
| 1 | Skoog, West, Holler, Crouch. 2004; Analitik Kimya Temel İlkeler, Türkçe Çeviri Ed. Esma KILIÇ, Hamza YILMAZ, 8. Baskı, Bilim Yayıncılık, Ankara | | | |
| 1 | Daniel C. Harris; Nicel Kimyasal Analiz, Türkçe Çeviri Ed. Ali Rehber TÜRKER, 1. Baskı, Palme Yayınevi, Ankara | | | 2 | Gündüz, T. 1984; Kalitatif Analiz Ders Kitabı, 7. Baskı, Gazi Yayınevi, Ankara | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 14.04.2020 | 1,5 | 50 | | End-of-term exam | 16 | 06.06.2020 | 1,5 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 4 | 14 | 56 | | Sınıf dışı çalışma | 3 | 14 | 42 | | Arasınav için hazırlık | 5 | 2 | 10 | | Arasınav | 1.5 | 1 | 1.5 | | Uygulama | 1 | 10 | 10 | | Ödev | 1 | 8 | 8 | | Dönem sonu sınavı için hazırlık | 8 | 3 | 24 | | Dönem sonu sınavı | 1.5 | 1 | 1.5 | | Total work load | | | 153 |
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