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| KIM4031 | Measurement and Evaluation in Chemistry | 2+0+0 | ECTS:4 | | Year / Semester | Fall Semester | | Level of Course | First Cycle | | Status | Elective | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | Face to face | | Contact Hours | 14 weeks - 2 hours of lectures per week | | Lecturer | Prof. Dr. Celal DURAN | | Co-Lecturer | Prof. Dr. Ömer Dalman | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | Comprehend error sources in chemical analysis.
Give basic information about the processing and evaulation of statical data.
To report the results of the analysis validation and validation parametres comprehand.
Provide basic information for comparison of standartization and calibration terms and calibration methods
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| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | İnterpet errors and major error sources in chemical analysis | 1,2,3,4,5,6,7,8 | 1 | | LO - 2 : | Evaulate the analytical and statical data | 1,2,3,4,5,6,7,8 | 1 | | LO - 3 : | Will be able to use calculators and computers in statical calculations | 1,2,3,4,5,6,7,8 | 1 | | LO - 4 : | Will be able to define and calculate terms of accuracy,precision,standart deviation,variance,significant figure,spread.confidence level.confidence interval | 1,2,3,4,5,6,7,8 | 1 | | LO - 5 : | İnterpet the effects of systematic and random errors on analytical results | 1,2,3,4,5,6,7,8 | 1 | | LO - 6 : | Will be able to compare and interpet on experimental value with a known value | 1,2,3,4,5,6,7,8 | 1 | | LO - 7 : | Will be able to check the quality of experimental measurement | 1,2,3,4,5,6,7,8 | 1 | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| Accuarcy and precision in analysis.Fault and major sources in chemical analysis.Random errors in chemical analysis.Statitical evaluation of random error.Examination of systematic faults.Random and systematic faults in titrimetric analysis.Errors in quantitative analysis.Calculators and computers in statical calculations.Quality control and sampling.Mistakae in instrümental analysis standartization and calibration.Comparison of calibartion methods.
Reproducibility and variance analysis.
Performance of analytical methods. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Errors in chemical analysis. Statistics of repetitive measurements. examination of random and systematic faults and statistical evaluation. | | | Week 2 | Errors in chemical analysis. Statistics of repetitive measurements. examination of random and systematic faults and statistical evaluation. | | | Week 3 | Errors in chemical analysis. Statistics of repetitive measurements. examination of random and systematic faults and statistical evaluation. | | | Week 4 | Errors in chemical analysis. Statistics of repetitive measurements. examination of random and systematic faults and statistical evaluation. | | | Week 5 | Errors in chemical analysis. Statistics of repetitive measurements. examination of random and systematic faults and statistical evaluation. | | | Week 6 | Errors in quantitative and titrimetric analysis. | | | Week 7 | Errors in instrumental analysis. | | | Week 8 | Exam | | | Week 9 | Quality control, sampling and quality control cards. | | | Week 10 | Standardization and calibration. | | | Week 11 | Comparison of calibration methods. | | | Week 12 | Correction of systematic errors during calibration. | | | Week 13 | Validation and validation parameters. | | | Week 14 | Kimyasal hesaplamalarda anlamlı rakamlar, anlamlı rakamların yuvarlanması, analiz sonuçlarının rapor edilmesi. | | | Week 15 | Processing and evaluation of statistical data. | | | Week 16 | Exam | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 13/11/2017 | 90 | 50 | | End-of-term exam | 16 | 02/01/2018 | 90 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 2 | 14 | 28 | | Sınıf dışı çalışma | 2 | 14 | 28 | | Arasınav için hazırlık | 4 | 1 | 4 | | Arasınav | 2 | 1 | 2 | | Dönem sonu sınavı için hazırlık | 2 | 8 | 16 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 80 |
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