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FACULTY of SCIENCE / DEPARTMENT of CHEMISTRY /
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KIM4001Analytical Separation Methods2+0+0ECTS:4
Year / SemesterFall Semester
Level of CourseFirst Cycle
Status Elective
DepartmentDEPARTMENT of CHEMISTRY
Prerequisites and co-requisitesNone
Mode of DeliveryFace to face
Contact Hours14 weeks - 2 hours of lectures per week
LecturerProf. Dr. Hakan ALP
Co-LecturerProf.Dr. Celal DURAN
Language of instructionTurkish
Professional practise ( internship ) None
 
The aim of the course:
To teach the separation methods that are particularly used to eliminate the effect of interfering species before the analysis.
 
Learning OutcomesCTPOTOA
Upon successful completion of the course, the students will be able to :
LO - 1 : know the fundamentals and importance of separation chemistry
LO - 2 : know the name of analytical separation methods
LO - 3 : evaluate the chromatographic data
LO - 4 : know the fundamentals of high performance liquid chromatography
LO - 5 : know the fundamentals of gas chromatography
LO - 6 : know the advantage of supercritical fluid chromatography
LO - 7 : know the fundamentals of electrophoresis
CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome

 
Contents of the Course
Classification of separation methods Extraction Introduction to chromatography Liquid chromatography Gas chromatography Supercritical fluid chromatography Electrophoreses
 
Course Syllabus
 WeekSubjectRelated Notes / Files
 Week 1Classification of analytical separation methods
 Week 2Extraction, distilation, precipitation separations
 Week 3Defination of chromatography and general aspects
 Week 4Factors effecting separation yields
 Week 5Principles of qualitative and quantitative analysis by chromatographic methods
 Week 6Principle of high pressure liquid chromatography
 Week 7Colons in high pressure liquid chromatography
 Week 8Detectors in high pressure liquid chromatography
 Week 9Mid-term exam
 Week 10Principle of gas chromatography
 Week 11Colons in gas chromatography
 Week 12Detectors in gas chromatography
 Week 13Applications of gas chromatography
 Week 14Applications of supercritical fluid chromatography
 Week 15Electrophoresis
 Week 16Electrophoresis
 
Textbook / Material
 
Recommended Reading
 
Method of Assessment
Type of assessmentWeek NoDate

Duration (hours)Weight (%)
Mid-term exam 9 15/11/2017 1 50
End-of-term exam 16 10/01/2018 1 50
 
Student Work Load and its Distribution
Type of workDuration (hours pw)

No of weeks / Number of activity

Hours in total per term
Yüz yüze eğitim 2 14 28
Sınıf dışı çalışma 4 10 40
Arasınav için hazırlık 2 9 18
Arasınav 2 1 2
Dönem sonu sınavı için hazırlık 2 6 12
Dönem sonu sınavı 2 1 2
Total work load102