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| KIM2007 | Analytical Chemistry Laboratory - I | 0+0+3 | ECTS:4 | | Year / Semester | Fall Semester | | Level of Course | First Cycle | | Status | Compulsory | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | Lab work , Practical | | Contact Hours | 14 weeks - 3 hours of laboratory per week | | Lecturer | Prof. Dr. Ümmühan TURGUT OCAK | | Co-Lecturer | PROF. DR. Hakan ALP,PROF. DR. Ömer DALMAN, | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | The students should obtain knowledge about application of Qualititative Analysis Methods |
| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | separate and determinate cations and anions
| 2,3,4,5,6,7,8 | 1,4 | | LO - 2 : | carry out heating, decantation, centrufuging.
| 2,3,4,5,6,7,8 | 1,4 | | LO - 3 : | carry out precipitation and filtration.
| 2,3,4,5,6,7,8 | 1,4 | | LO - 4 : | determine cation and anion groups.
| 2,3,4,5,6,7,8 | 1,4 | | LO - 5 : | carry out gravimetric analysis.
| 2,3,4,5,6,7,8 | 1,4 | | LO - 6 : | carry out analysis of real samples.
| 2,3,4,5,6,7,8 | 1,4 | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| Analysis of Group 1 Cations (Pb, Ag, Hg- (I) ) , Analysis of Group 2 Cations (Cu, Cd, Bi, Hg- (II) , As, Sb, Sn) , Analysis of Group 3 Cations (Fe, Al, Cr, Ni, Co, Mn, Cn) , Analysis of Group 4 Cations (Ba, Sr, Ca, Mg) , Analysis of Group 5 Cations (Na, K, NH4) , Analysis of Group 1 Anions (CO32-, PO43-, BO2-, SO42-, SO32-) , Analysis of Group 2 Anions (I-, Br-, NO3-, CH3COO-, S2O32-, SCN-) , Chapter 8 Analysis of Cations and Anions in Solid Sample (Complete Analysis) .
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Introduction
| | | Week 2 | Analysis of Group I Cations | | | Week 3 | Analysis of Group I-V Cations | | | Week 4 | Analysis of Group I-V Cations | | | Week 5 | Analysis of Group I-V Cations | | | Week 6 | Analysis of Group I-V Cations | | | Week 7 | Analysis of Anions | | | Week 8 | Gravimetric Ni Analysis | | | Week 9 | Exam | | | Week 10 | Gravimetric Fe Analysis | | | Week 11 | Gravimetric Ba Analysis | | | Week 12 | Completion of Experiments | | | Week 13 | Make up Experiments | | | Week 14 | Make up Experiments | | | |
| 1 | Analitik Kimya-I Laboratuarı Notları, Fen Fakültesi, Kimya Bölümü, KTÜ Yayınları, Trabzon | | | |
| 1 | Gündüz, T. 2007; Yarı Mikro Kalitatif Analiz, Gazi Kitabevi, Ankara | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 19.11.2016 | 2 | 50 | | End-of-term exam | 16 | 13.01.2017 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 0 | 0 | 0 | | Sınıf dışı çalışma | 0 | 0 | 0 | | Laboratuar çalışması | 3 | 13 | 39 | | Arasınav için hazırlık | 7 | 5 | 35 | | Arasınav | 2 | 1 | 2 | | Uygulama | 0 | 0 | 0 | | Klinik Uygulama | 0 | 0 | 0 | | Ödev | 0 | 0 | 0 | | Proje | 0 | 0 | 0 | | Kısa sınav | 2 | 5 | 10 | | Dönem sonu sınavı için hazırlık | 10 | 4 | 40 | | Dönem sonu sınavı | 2 | 1 | 2 | | Diğer 1 | 0 | 0 | 0 | | Diğer 2 | 0 | 0 | 0 | | Total work load | | | 128 |
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