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| ECZ2024 | Analytical Chemistry II-Lab. | 0+0+3 | ECTS:2 | | Year / Semester | Spring Semester | | Level of Course | Second Cycle | | Status | Compulsory | | Department | DEPARTMENT of PHARMACEUTICS | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of laboratory per week | | Lecturer | Prof. Dr. Dilek KUL | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | In addition to volumetric and gravimetric analysis, it aims to teach widely used instrumental methods and the use of devices. |
| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | Learns quantitative analysis with age and instrumental analysis methods. | 1,4,5 | 1,4, | | LO - 2 : | Have theoretical and applied knowledge and skills in the field of Analytical Chemistry. | 1,4,5 | 1,4, | | LO - 3 : | Learns method development in chemical analysis and how to validate the developed method, validation parameters. | 1,4,5 | 1,4, | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| Adjusting Standard Solutions; Volumetric Quantification; Gravimetric Quantification; Potentiometric Measurement; Analysis with Voltammetric Methods; Analysis with Spectroscopic Methods; Separation by Chromatographic Methods. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Preparation and Adjustment of Standard Solutions | | | Week 2 | Quantification of Aspirin and Boric Acid by Volumetric Method | | | Week 3 | Determination of Calcium Carbonate and Acetic Acid by Volumetric Method, Permangonometric Determination of Hydrogen Peroxide | | | Week 4 | Complexometric Titration, Determination of Ca and Mg | | | Week 5 | Potentiometric Acid-Base Titration | | | Week 6 | Determination of Sulphate by Gravimetric Method | | | Week 7 | Determination of Sulphate by Gravimetric Method | | | Week 8 | Quantification by UV-Vis Spectrophotometry | | | Week 9 | Midterm exam | | | Week 10 | Potentiometric / Voltammetric Devices and Analysis Methods | | | Week 11 | Infrared Spectrometry Device and Its Use, Nuclear Magnetic Resonance Spectrometry Device and Its Use | | | Week 12 | Separation and Quantification by Gas Chromatography | | | Week 13 | Separation and Quantification by High Pressure Liquid Chromatography | | | Week 14 | Experiment Compensation Week | | | Week 15 | Experiment Compensation Week | | | Week 16 | Final Exam | | | |
| 1 | Analitik Kimya-II Laboratuvar Föyü | | | |
| 1 | D.A. Skoog, F.J. Holler, T.A. Nieman (Eds.), Enstrümental Analiz İlkeleri, Çeviri Editörleri: E. Kılıç, F. Köseoğlu, H. Yılmaz, Bilim yayıncılık, Ankara, 2013. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 17/04/2024 | 1 | 50 | | End-of-term exam | 16 | 07/06/2024 | 1 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Laboratuar çalışması | 3 | 14 | 42 | | Arasınav için hazırlık | 1 | 5 | 5 | | Arasınav | 1 | 1 | 1 | | Dönem sonu sınavı için hazırlık | 1 | 5 | 5 | | Dönem sonu sınavı | 1 | 1 | 1 | | Total work load | | | 54 |
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