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| ECZ4039 | Pharmacognosy Laboratory - III | 0+0+3 | ECTS:2 | | Year / Semester | Fall Semester | | Level of Course | Second Cycle | | Status | Compulsory | | Department | DEPARTMENT of PHARMACEUTICS | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of laboratory per week | | Lecturer | Prof. Dr. Ufuk ÖZGEN | | Co-Lecturer | Research Assistant Tuğba SUBAŞ | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | To give theoretical knowledge and practice about alkaloids, identification of alkaloids; microscopic analysis of alkaloids; quantification of alkaloids; tropane alkaloids and related drugs; quinoline alkaloids and related drugs; opium alkaloids and related drugs; purine alkaloids and related drugs; saponosides and related drugs; cardioactive heterosides and related drugs; Analysis of herbal tea |
| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | Know alkaloids and identification of the alkaloids
| 2,3 | 1,4, | | LO - 2 : | Know Tropane alkaloids and tropane alkaloid-containing plants related drugs; Quinoline alkaloids and quinoline-containing plants | 2,3 | 1,4, | | LO - 3 : | Know Opium alkaloids and opium alkaloid-containing plants; Purine alkaloids and recognize purine alkaloid-containing plants | 2,3 | 1,4,5, | | LO - 4 : | Knows Cardioactive heterosides and cardioactive heterosides-containing plants related drugs; Saponosides and saponosides-containing plants; Knows analysis of herbal tea | 2,3 | 1,4,5, | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| General information about alkaloids, Alkaloid recognition reactions; Microscopic analysis of alkaloids; Quantification of alkaloids; Tropane alkaloids and related drugs; Quinoline alkaloids and related drugs; Opium alkaloids and related drugs; Purine alkaloids and related drugs; Saponosides and related drugs; Cardioactive heterosides and related drugs; Analysis of herbal tea |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Demonstration (Alkaloids-general) | | | Week 2 | Microscopical Analysis of Poppy Fruit (Papaveris fructus) | | | Week 3 | Detection of Alkaloids from Plant Materials
| | | Week 4 | Detection of Solanaceae Alkaloids | | | Week 5 | Detection of Cortex Chinae Alkaloids and Determination of Total Alkaloids of Cortex Chinae | | | Week 6 | Detection and Determination of Opium Alkaloids
| | | Week 7 | Detection of Xanthine Alkaloids
| | | Week 8 | Caffeine from tea and Pharmacopeial Analysis of Caffeine | | | Week 9 | Midterm | | | Week 10 | Analysis of Herbal Tea | | | Week 11 | Quantitative Determination of Caffeine by HPLC Technique | | | Week 12 | Homework presentations I | | | Week 13 | Homework presentations II | | | Week 14 | Homework Presentation III
| | | Week 15 | Compensation week | | | Week 16 | Exam | | | |
| 1 | Sakar, M.K., Tanker, M. 1991. Fitokimyasal Analizler: Tanım, Miktar Tayini ve İzolasyon, Ankara Üniversitesi Eczacılık Fakültesi Yayınları, No 67, Ankara | | | |
| 1 | Tanker, M., Tanker, N. 1990; Farmakognozi Cilt 2, Ankara Üniversitesi Eczacılık Fakültesi Yayınları, No 65, Ankara | | | 2 | Tanker, M., Tanker, N. 1991; Farmakognozi Cilt 1, Ankara Üniversitesi Eczacılık Fakültesi Yayınları, No 66, Ankara | | | 3 | Trease and Evans, 1996; Pharmacognosy, London | | | 4 | Hänsel,R., Sticher, O., Steinegger, E. 1999; Pharmakognosie, Springer-Verlag, Berlin | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 29/11/2023 | 1 | 35 | | Laboratory exam | 2
3
4
5
6
7
8
10 | 10/10/2023
17/10/2023
24/10/2023
31/10/2023
07/11/2023
14/11/2023
21/11/2023
05/12/2023 | 1 | 15 | | Presentation | 12
13
14 | 19/12/2023
26/12/2023
02/01/2024 | 1 | 15 | | End-of-term exam | 16 | 05/01/2024 | 2 | 35 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 1 | 3 | | Laboratuar çalışması | 3 | 10 | 30 | | Arasınav için hazırlık | 10 | 1 | 10 | | Arasınav | 1 | 1 | 1 | | Ödev | 1 | 3 | 3 | | Dönem sonu sınavı için hazırlık | 10 | 1 | 10 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 59 |
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