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| KIM 413 | Industrial Chemistry Laboratory - I | 0+0+4 | ECTS:4 | | Year / Semester | Fall Semester | | Level of Course | First Cycle | | Status | Compulsory | | Department | DEPARTMENT of CHEMISTRY | | Prerequisites and co-requisites | None | | Mode of Delivery | Lab work | | Contact Hours | 14 weeks - 4 hours of laboratory per week | | Lecturer | Doç. Dr. Ümit DEMİRBAŞ | | Co-Lecturer | Lecturers in Inorganic Chemistry Division | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | The objectives of the course are to teach how the analysis of some important industrial material can be analyzed, purpose of the analysis, what the chemical the reaction are, the methods of the analysis, calculation of the results and interpretation of the results, how the related problems are solved. |
| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | do coal and oil analysis such as moisture, flying material, raw coke, ash, and burnable sulfur in a example of coal, determine the heat of coal, to measure viscosity, flash point, density and flowing point of oils. | 2,3,4,5,6,7,8 | 1,4 | | LO - 2 : | do vegatable oil analysis including calculation of oil% in a example of seed, acid, soaping, iodine and peroxide indexes. | 2,3,4,5,6,7,8 | 1,4 | | LO - 3 : | do fertilizer analysis such as the determination of nitrogen amount of nitrogen containing fertilizers and percentage of P2O5 in phosphors containing fertilizers. | 1,2,3,4,5,6,7,8 | 1,4 | | LO - 4 : | explain the kinds of soap, how they are produced, determination of free alkality, free fat acid, determination of chloride and total active material in detergents. | 2,3,4,5,6,7,8 | 1,4 | | LO - 5 : | explain production of cement, calculation the percentages of SiO2, R2O3, SO3, CaO and MgO in a sample. | 2,3,4,5,6,7,8 | 1,4 | | LO - 6 : | do water analysis such as hardiness, soap and EDTA tests, determination of the type and amount of alkality, amount of chloride, amount of organic compound | 2,3,4,5,6,7,8 | 1,4 | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| Fuels and Analysis of them: How should a coal example be taken, preparation of a example of coal for analysis, determination of moisture, flying material, raw coke, burnable sulfur, ash and heat of a coal example, determination of viscosity, flash point, flowing point and density of an oil example. Analysis of vegetable oils: A brief information about production of a vegetable oil, determination of acid, soaping, iodine and peroxide indexes in vegetable oils, extraction of oil from hazelnut and determination of percentage of oil in the hazelnut. Fertilizers and Analysis of them: Preparation of a fertilizer for analysis, determination of nitrogen in nitrogen containing fertilizers by distillation and formaldehyde solution, determination of %P2O5 in phosphorus containing fertilizers, the reactions in the experiments. Analysis of Soap and Detergent: Determination of free alkality, free fat acid, determination of chloride and total active component in detergents. . Analysis of cement and Lime: Determination of SiO2, SiO2 and insoluble component in acid, R2O3, SO3 , CaO and MgO in a cement, determination of mass loss of lime by heating. Water Analysis: Taking an sample of water for analysis, determination of total hardness of water by soap and EDTA solutions, determination of permanent and temporary hardness in different units, amounts of alkality, chloride, iron and organic component in a water sample. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | General information about the experiment, determination of the groups, distribution of the equipments requıred for the experiments to the students | | | Week 2 | Analysis of water: determination of alkality, total and temperary hardness by different methods in water. | | | Week 3 | Determination of chloride and total organic sabstance in water | | | Week 4 | Analysis of Coal. Determination of raw coak, coak, water, flying material, ash and burneble sulfer in a coal sample. | | | Week 5 | Determination of specific heat of a soli or liquid fuel, viscosity,flash point and flowing point of a fuel oil sample | | | Week 6 | Analysis of Cement and Lime: Determinatin of heating lost, amount of CaO, MgO in a cement or lime sample.
| | | Week 7 | Determination of percentage of insoluble sabstance into acid, SiO2, SO3 and R2O3 in sample of cement | | | Week 8 | Analysisi of Fertilizers: Determination of total and ammonia nitrogen in a nitrogen containing fertilizer using different methods. | | | Week 9 | Mid-term Exam | | | Week 10 | Determination of percentage of P2O5 in a phosphrous containing fertilizer | | | Week 11 | Analysis of Eatable oils: Determination of acid, soaping indexes in a vegetable oil. | | | Week 12 | Production of oil from hazelnut, Determination of iodine and peroxide indexes in a vegetale pil | | | Week 13 | Production of soap, determination of free alkality and acidity in a soap sample | | | Week 14 | Determination of total active sabatance and chloride in sample of detergent sample | | | Week 15 | Make-up experiments | | | Week 16 | End-of-term exam | | | |
| 1 | Alpar,S.R., Hakdiyen, İ., Bigat, T. 1976; Sınai Kimya Analiz Metotlar, İÜ Yayınları, No 2127, İstanbul | | | |
| 1 | Basin, S., İmren, D.,Yüce, S. 2001; Kimyasal Teknolojiler ve Analizler, CÜ Yayınları, No 87, Sivas | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 11/11/2015 | 2 | 50 | | Laboratory exam | 3
5
7
11
13 | 11/10/2015
1/11/2015
15/11/2015
6/12/2015
20/12/2015 | | | | End-of-term exam | 17 | 20/01/2016 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Laboratuar çalışması | 4 | 14 | 56 | | Arasınav için hazırlık | 2 | 5 | 10 | | Arasınav | 2 | 1 | 2 | | Kısa sınav | 2 | 10 | 20 | | Dönem sonu sınavı için hazırlık | 2 | 5 | 10 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 100 |
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