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| ECZ2046 | Analytical Chemistry II-Lab. | 0+0+3 | ECTS:2 | | Year / Semester | Spring Semester | | Level of Course | Second Cycle | | Status | Compulsory | | Department | DEPARTMENT of PHARMACEUTICS | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of laboratory per week | | Lecturer | Prof. Dr. Dilek KUL | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | The purpose of this course is to provide practical instruction in volumetric and gravimetric analysis, as well as the use of some instrumental devices. |
| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | They reinforce their theoretical knowledge by applying it in the laboratory. | 1 - 4 - 5 | 1,4, | | LO - 2 : | They will also learn how to use chemicals, glassware, and other materials in the laboratory and what precautions to take while performing volumetric and gravimetric methods. | 1 - 4 - 5 | 1,4, | | LO - 3 : | They will learn some commonly used electrochemical, spectroscopic, and chromatographic instruments and how to use them. | 1 - 4 - 5 | 1,4, | | LO - 4 : | They will be able to work as a team in the laboratory. | 1 - 4 - 5 | 1,4, | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| Calibration of Standard Solutions; Volumetric Quantification; Gravimetric Quantification; Quantification by UV-Vis Spectroscopy; Potentiometric Measurement; Voltammetric Quantification; Separation by Chromatographic Methods. |
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| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Preparation and Calibration of the Standard Solutions | | | Week 2 | Determination of Amount of Aspirin and Boric Acid by Volumetric Method | | | Week 3 | Calcium Carbonate and Acetic Acid Amount Determination by Volumetric Method, Permangonometric Hydrogen Peroxide Determination | | | Week 4 | Complexometric Titration, Ca and Mg Determination | | | Week 5 | Potentiometric Acid-Base Titration | | | Week 6 | Sulphate Determination by Gravimetric Method | | | Week 7 | Sulphate Determination by Gravimetric Method | | | Week 8 | Quantification by UV-Vis Spectrometry | | | Week 9 | Mid-term Exam | | | Week 10 | Separation by Gas Chromatography (GC) and Quantification | | | Week 11 | Separation by High Pressure Liquid Chromatography (HPLC) and Quantification | | | Week 12 | Nuclear Magnetic Resonance Spectrometer (1H-NMR) and Spectrums | | | Week 13 | Qualitative and Quantitative Determination by Voltametric Methods using A Potentiostat Device | | | Week 14 | Experiment Compensation Week | | | Week 15 | Experiment Compensation Week | | | Week 16 | Final Exam | | | |
| 1 | D.A. Skoog, F.J. Holler, T.A. Nieman (Eds.), Enstrümental Analiz İlkeleri, Çeviri Editörleri: E. Kılıç, F. Köseoğlu, H. Yılmaz, Bilim yayıncılık, Ankara, 2013. | | | |
| 1 | Analitik Kimya Laboratuvar Notları. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 09/04/2026 | 2 | 50 | | End-of-term exam | 16 | 11/06/2026 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Laboratuar çalışması | 3 | 14 | 42 | | Arasınav için hazırlık | 1 | 8 | 8 | | Arasınav | 2 | 1 | 2 | | Dönem sonu sınavı için hazırlık | 1 | 5 | 5 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 59 |
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