|
|
| ECZ2025 | Analytical Chemistry - I | 3+0+0 | ECTS:4 | | Year / Semester | Fall Semester | | Level of Course | Second Cycle | | Status | Compulsory | | Department | DEPARTMENT of PHARMACEUTICS | | Prerequisites and co-requisites | None | | Mode of Delivery | | | Contact Hours | 14 weeks - 3 hours of lectures per week | | Lecturer | Doç. Dr. Fatma AĞIN | | Co-Lecturer | | | Language of instruction | Turkish | | Professional practise ( internship ) | None | | | | The aim of the course: | | This course aims to teach how to perform solution calculations, all volumetric and gravimetric titrations, and related calculations. |
| Learning Outcomes | CTPO | TOA | | Upon successful completion of the course, the students will be able to : | | | | LO - 1 : | Performs solution preparation calculations. Uses buffer solutions. | 1 - 5 | 1, | | LO - 2 : | Learns classical analysis methods (volumetric and gravimetric) and makes calculations. | 1 - 5 | 1, | | LO - 3 : | Obtains quantitative and qualitative information about the analyte of interest by drawing titration curves. | 1 - 5 | 1, | | LO - 4 : | Makes and prepares all necessary calculations for all solutions required in experimental studies. | 1 - 5 | 1, | | CTPO : Contribution to programme outcomes, TOA :Type of assessment (1: written exam, 2: Oral exam, 3: Homework assignment, 4: Laboratory exercise/exam, 5: Seminar / presentation, 6: Term paper), LO : Learning Outcome | | |
| Intramolecular and intermolecular bonds; Concentration units; Aqueous solutions and chemical equilibrium (buffers, sparingly soluble salts, activity); Gravimetric analysis methods; Neutralization titrations; Complexation titrations; Electrochemical methods
|
| |
| Course Syllabus | | Week | Subject | Related Notes / Files | | Week 1 | Intramolecular and intermolecular bonds, Concentration units | | | Week 2 | Aqueous solutions, Chemical equilibrium, Ionization of water, Solubility of very and slightly soluble salts | | | Week 3 | Solubility of sparingly soluble salts, Acid-base ionization constants, Buffer solutions | | | Week 4 | Properties of buffer solutions, Alpha values of buffers, Buffer capacity, Preparation of buffer solutions, Effect of electrolytes on chemical equilibrium, Activity, Debye-Hückel equation | | | Week 5 | Effect of foreign ions on poorly soluble salts, Solution of equilibrium problems in complex systems, Mass and charge balances, Problems involving multiple equilibria | | | Week 6 | Controlled selective precipitation, Precipitation gravimetry and calculations | | | Week 7 | Standard solutions, Back titration, Gravimetric titrimetry, Precipitation titration curves | | | Week 8 | Argentometric methods, Neutralization titrations, Acid-base indicators, Strong acid-base titration curves | | | Week 9 | Mid-term exam | | | Week 10 | Weak acid-base titration curves, Co-hydrolysis of anion and cation, Polyprotic acids and buffer solutions | | | Week 11 | Titration curves of polyprotic systems, ionization and titration curve of sulfuric acid, pH calculation of acid solution mixtures | | | Week 12 | Complexation titrations, Formation constants, EDTA and titrations, indicators of EDTA titrations, Water hardness | | | Week 13 | Oxidation/Reduction reactions, Electrochemical cells, Electrode potentials, Nernst equation | | | Week 14 | Calculation of cell potentials, Redox titrations | | | Week 15 | Redox indicators, Potentiometry (Reference and Indicator electrodes), Potentiometric titrations | | | Week 16 | Final exam | | | |
| 1 | Analitik Kimya-I Ders Notları | | | |
| 1 | D.A. Skoog, D.M. West, F.J. Holler, S.R. Crouch, (Eds. Prof. Dr. E. Kılıç, Prof. Dr. H. Yılmaz), Analitik Kim ya Temel İlkeler, 8. Baskı, Bilim Yayıncılık, Ankara, 2004. | | | 2 | D.D. Harris, Nicel Kimyasal Analiz, Çeviri: A.R. Türker, Palme Yayıncılık, Ankara, 2015. | | | |
| Method of Assessment | | Type of assessment | Week No | Date | Duration (hours) | Weight (%) | | Mid-term exam | 9 | 19/11/2025 | 2 | 50 | | End-of-term exam | 16 | 07/01/2026 | 2 | 50 | | |
| Student Work Load and its Distribution | | Type of work | Duration (hours pw) | No of weeks / Number of activity | Hours in total per term | | Yüz yüze eğitim | 3 | 14 | 42 | | Arasınav için hazırlık | 4 | 8 | 32 | | Arasınav | 2 | 1 | 2 | | Dönem sonu sınavı için hazırlık | 4 | 6 | 24 | | Dönem sonu sınavı | 2 | 1 | 2 | | Total work load | | | 102 |
|